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双波长薄层扫描测定赤芍总甙中芍药甙含量 被引量:6

Determination of Paeoniflorin in Total Saponins of Radix Paeoniae Rubra by TLC Scanning
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摘要 目的 :研究赤芍总甙的制备工艺和质量标准。方法 :赤芍经乙醇回流 ,乙醚脂和正丁醇萃取得到赤芍总甙 ,得率 >5 % ,所得赤芍总甙以双波长薄层扫描测定了芍药甙含量 ,测定波长λS=2 5 4nm。结果 :样品中芍药甙含量平均为 44.1%。结论 :该提取方法简便、快速、可行。 Objective: To study the preparing technology of total saponins of Radix Paeoniae Rubra and its quality standards. Methods: Total saponins were extracted from Paeonia lactiflora Pall. by EtOH refluxing, EtO degreasing and n BuOH extracts, the yield was more than 5%. The dual wavelength TLC scanning was used to determine the content of paeoniflorin at 254 nm. Results: The average content of paeoniflorin in the extractive was 44.1%. Conclusion: The extracting method was simple, rapid and available.
出处 《时珍国医国药》 CAS CSCD 2001年第1期25-26,共2页 Lishizhen Medicine and Materia Medica Research
关键词 赤芍总甙 提取 芍药甙 含量 测定 薄层扫描 中药 Total saponins of paeonia Extraction Paeoniflorin Determination TLC scanning
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