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应用原子吸收光谱测定蜂蜜中铁的研究 被引量:2

Study of Determination of Iron in Honey by Atomic Absorption Spectrometry
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摘要 本实验利用火焰原子吸收法测定蜂蜜中的铁。测量波长2483nm,狭缝02nm,灯电流5.0mA,空气流量10.0L/min,乙炔流量2.00L/min。样品经消解或灰化(550℃)等处理后导入火焰测定吸光度,与标准系列比较定量。测得蜂蜜样品中铁含量为40.3μg/ml,RSD%=1.29,回收率=100.4%。 Iron in honey was detetrined by flame atothecabsorbing spectrometry method in this study.Wavelength 248. 3 nm, narrow 0. 2nm, lamp current5. 0mA, air flux 10. 0 L/min, acetylene flux 2. 00L/min. Samples were determined after being cleared up or incraerated, and were comared with standard seriet. The content of iron in honey sample is 40.3μg/ml, RSD% = 1 .29, Recovery = 100 .4%.
作者 安宝强
出处 《养蜂科技》 1999年第6期2-6,共5页 Apicultural Science and Technology
关键词 蜂蜜 营养成分 原子吸收光谱 flame atomic absorption spectrometry honey iron
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  • 1付文燕.微波消解等离子体发射光谱法测定蜂蜜中的Zn[J].现代预防医学,2004,31(6):884-884. 被引量:1
  • 2李敬慈,丁天惠.高效液相色谱法分析蜂蜜中的糖[J].分析测试学报,1995,14(5):62-65. 被引量:17
  • 3黄彩娇.湿法消解-火焰原子吸收法测定蜂蜜中的锌[J].海峡预防医学杂志,2006,12(3):45-46. 被引量:6
  • 4黄伟坤.食品检验与分析[M].中国轻工业出版社,1995..
  • 5Jimenez J J. Determination of rotenone residues in raw honey by solid - phase extraction and high - permance liquid chromatography [J] . Journal of chromatography A, 2000, 871:67-73 .
  • 6Jimenez J J. Solid - phase microextraction applied to the analysis of pesticide residues in honey using gas chromatography with electron - capture detection [ J] . Journal of chromatography A,1998, 829: 269- 277.
  • 7Jimenez. Gas chromatography with electron - capture and nitrogen- phosphorus detection in the analysis of pesticides in honey after elution from a florisil column [ J] . Journal of chromatographyA, 1998, 823: 381-387.
  • 8Korta. Study of semi - automated solid - phase extraction for the determination of acaricide residues in honey by liquid chromatograghy [J] . Journal of chromatography A, 2001, 930:21 -29.
  • 9Edder. Determination of streptomycin residues in food by solid phase extraction and liquid chromatography with post - column derivatization and fluorometric detection [J] . Jourmal of chromatography A [J], 1999, 830: 345- 351.
  • 10Campos. Characterisation of flavonoids in three hive products bee propolisand honey [J] . Planta medica, 1990, 56: 580-581.

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