摘要
对二甲苯与N-溴代丁二酰亚胺反应合成对二溴甲基苯,后者与乙酰丙酮反应合成1,4-二(2',2'-二乙酰基乙烷基)苯,再与取代苯胺反应,较高收率合成了5种新型的苯二亚甲基桥联的双β-酮亚胺化合物;并通过1HNMR、IR和元素分析对产物进行了表征.
Five novel xylylene-bridged his （β-ketoiminate） compounds were synthesized with high yields by substituted anilines reacted with 1, 4-（ 2＇, 2＇-acetonyethyl ） benzene which was synthesized with acetylacetone and p- dibromomethylbenzene prepared with p-Xylene and NBS. All the title compounds reported were characterized by 1H NMR, IR and elemental analysis.
出处
《中南民族大学学报（自然科学版）》
CAS
2013年第2期26-28,共3页
Journal of South-Central University for Nationalities：Natural Science Edition
基金
国家自然科学基金资助项目(21172269
40830852)
