摘要
以预氧化纤维网胎为原料,经过接力层叠针刺工艺制备的预氧化纤维整体毡为预制体,在不同的炭化条件下得到炭纤维整体毡,并以热固性树脂为先驱体,采用浸渍—固化—树脂炭化—石墨化的方法制备了硬质隔热用炭纤维整体毡。研究了针刺工艺、炭化温度、浸渍液浓度和固化时所加压力等因素对材料密度的影响,并借助扫描电镜观察样品的微观结构。结果表明:采用高的针刺密度和针刺深度参数,得到的预制体密度较大;炭化温度对整体毡密度的影响不大,但其含碳量随炭化温度变化明显;浸渍液浓度及预制体密度均对硬质毡的密度有一定影响;随着固化时压力的增大,样品的密度也逐渐提高。
With pre-oxidized fiber integrated felt prepared by relayed needle punching process as pre- form and thermosetting resin as precursor, impregnation-curing-carbonization of resin-graphitization process was employed to prepare rigid carbon fiber integrated felt used for thermal insulation. Effect of every process including needle punching parameters, carbonization temperature, solution concentra- tion and curing pressure on density was studied. Microstructure of samples was studied by using SEM. The results show that high values of needle-punching parameters lead to high values of preform density, carbonization temperature has little influence on density, but much influence on carbon con- tent. Also solution concentration and preform density have a certain influence on density. What is more, with increasing curing pressure, the density of samples increases.
出处
《材料工程》
EI
CAS
CSCD
北大核心
2013年第5期48-52,共5页
Journal of Materials Engineering
关键词
隔热材料
炭纤维整体毡
密度
影响因素
thermal insulation material
carbon fiber integrated felt
density
influence factor
