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Bi(25)FeO_40-g-C_3N_4磁性催化剂的制备及其可见光催化性能 被引量:6

Preparation of magnetic Bi(25)FeO_40-g-C_3N_4 catalyst and its high visible-light photocatalytic performance
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摘要 采用水热法制备了铁酸铋(Bi25FeO40),将其与类石墨相氮化碳(g-C3N4)复合得到Bi25FeO40-g-C3N4磁性光催化剂,用X-射线衍射(XRD)、扫描电子显微镜(SEM)、BET比表面积分析、UV-Vis光谱和磁滞回线对该磁性光催化剂进行了表征.考察了Bi25FeO40-g-C3N4复合催化剂对亚甲基蓝的可见光催化降解效果.结果表明,Bi25FeO40-g-C3N4复合催化剂对亚甲基蓝的可见光催化降解效率远高于Bi25FeO40.此外,Bi25FeO40-g-C3N4表现出顺磁性,可通过磁选分离并回收. Magnetic Bi25FeO40-g-C3N4 visible-light photocatalysts were prepared via the mixture and calcination of graphitic carbon nitrides (g-C3N4 ) and Bi25FeO40 synthesized by the hydrothermal methods. Bi25FeO40-g-C3N4 catalysts were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Brunauer- Emmett-Teller (BET) surface area analysis, UV-vis absorbance and magnetic hysteresis loop measurements. The results showed that Bi25FeO40-g-C3N4 composite photocatalyst exhibited prominently enhanced photocatalytic activity for the degradation of Methylene Blue (MB) under visible-light irradiation than that of Bi25FeO40. Additionally, the Bizs FeO40-g-C3 N4 composite was superparamagnetic, and could be readily recovered in an external magnetic field.
出处 《环境化学》 CAS CSCD 北大核心 2013年第5期748-754,共7页 Environmental Chemistry
基金 国家自然科学基金(51178223 51208257) 江苏省自然科学基金(SBK201240759) 江苏省环保科研课题(2012008)资助
关键词 Bi25FeO40-g-C3N4复合催化剂 可见光催化 磁分离 亚甲基蓝 Bi25FeO40-g-C3N4 photocatalyst, visible-light photocatalysis, magnetic separation, Methylene Blue.
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