摘要
提出了采用光电直读光谱法测定轧制态碳钢中碳、硅、锰、磷、硫、镍、铬、铜、钼、钒、铌、铝、硼、钙、钛、钨、铅、砷、锡、锑、锌等21种元素的含量。测定中选择氩气压力为0.7MPa,冲洗时间为5.0s,极距2.85mm。在优化的试验条件下,21种元素测定值的相对标准偏差(n=12)在0.3%～15%之间。方法用于线材和棒材实际样品分析,测定结果与化学分析方法的测定结果相一致。
Contents of C,Si,Mn,P,S,Ni,Cr,Cu,Mo,V,Nb,Al,B,Ca,Ti,W,Pb,As,Sn,Sb and Zn in samples of rolled carbon steel were determined by direct-reading spectrometry.Flow-rate and irrigation time of argon used in the determination were taken at 0.7 MPa and 5.0 s respectively,and electrode distance was taken at 2.85 mm.Under the optimized experimental conditions,values of RSD′s（n=12） of the 21 elements found were in the range of 0.3%-15%.The proposed method was applied to the analysis of wire and bar samples,and the results obtained were in conformity with those found by chemical method.
出处
《理化检验（化学分册）》
CAS
CSCD
北大核心
2013年第3期284-286,289,共4页
Physical Testing and Chemical Analysis(Part B:Chemical Analysis)
关键词
直读光谱法
轧制态碳钢
线材和棒材
元素
Direct-reading spectrometry
Rolled carbon steel
Wire and bar
Elements
