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PLS—近红外漫反射光谱法分析扑热息痛 被引量:1

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摘要 用常规和一阶导数近红外漫反射光谱法非破坏快速分析了粉末药品扑热息痛 ,比较了偏最小二乘 (PLS)法在两种情况的定量预测扑热息痛含量的能力 ,讨论了波长间隔对 PLS预测扑热息痛含量的影响。实验结果表明 ,在运用 PLS法前进行微分处理数据 ,没有产生明显的优点。
出处 《数理医药学杂志》 2000年第5期452-453,共2页 Journal of Mathematical Medicine
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  • 1Erk N, OEzkan Y, Banoglu E, et al. Simultaneous determination of paracetamol and methocarbamol in tablets by ratio spectra derivative spectrophotometry and LC [J]. Journal of Pharmaceutical and Biomedical Analysis, 2001, 24(3) : 469 -475.
  • 2Yiguang Tan, Zhiling Zhou, Peng Wang, et al. A study of a bio-mimetic recognition material for the BAW sensor by molecular imprinting and its application for the determination of paracetamol in the human serum and urine [J]. Talanta, 2001, 55(2) : 337 - 347.
  • 3Orlando Fatibello-Filho, Karina Omuro Lupetti, Iolanda Cruz Vieira. Chronoamperometric determination of paracetamol using an avocado tissue (Persea americana) biosensor [J]. Talanta, 2001, 55(4) :685 - 692.
  • 4Andres Criado, Soledad Cardenas, Mercedes Gallego, et al. Continuous flow spectrophotometric determination of paracetamol in pharmaceuticals following continuous microwave assisted alkaline hydrolysis [J]. Talanta, 2000, 53(2) : 417 - 423.
  • 5Erdal Dinc, Gamze KOkdil, Feyyaz Onur. Derivative ratio spectra-zero crossing spectmphotometry and LC method applied to the quantitative determination of paracetamol, propyphenazone and caffeine in ternary mixtures [J]. Journal of Pharmaceutical and Biomedical Analysis, 2001, 26(5-6): 769-778.
  • 6Alberto J. Nepote, Alejandro C. Olivieri. Simultaneous spectrofluorometric determination of oxatomide and phenylephrine in the presence of a large excess of paracetamol [J]. Anal Chimi Acta, 2001, 439(1): 87-94.
  • 7Easwaramoorthy D, Yu Yueh-Chuan, Huang Hsuan-Jung. Chemiluminescence detection of paracetamol by a luminol-permanganate based reaction [J]. Anal Chimi Acta, 2001, 439(1): 95- 100.
  • 8Murat Kartal. LC method for the analysis of paracetamol, caffeine and codeine phosphate in pharmaceutical preparations [J]. Journal of Pharmaceutical and Biomedical Analysis, 2001, 26(5 - 6) : 857 - 864.
  • 9陈新谦 金有豫.新编药物学 第14版[M].北京:人民卫生出版社,2000.231.
  • 10杨冰仪,莫金垣,杨晓云,王立世.高效毛细管电泳-安培法同时检测感冒药中的扑尔敏、扑热息痛和维生素C[J].色谱,1999,17(5):477-479. 被引量:8

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