摘要
在氯丁橡胶中加入环化试剂AlEt2 Cl-C6H5CH2 Cl,在 12 0℃× 2 0min条件下 ,可制备环化氯丁橡胶。借助IR ,1H -NMR ,DSC ,GPC和裂解色谱测试方法对产物进行了表征。结果表明 ,二甲苯溶剂参与了环化反应 ,且随环化度增加 ,参与反应的溶剂二甲苯的数目也逐渐增加 。
The cyclized CR was prepared by adding in cyclic agent AlEt 2Cl-C 6H 5CH 2Cl at 120℃×20min.The products were characterized with the aid of IR, 1H-NMR,DSC,GPC and So on.The result indicated that xylene solution participated in cyclic reaction,and increased with the increase of the degress of cyclization,and the polycyclic structure was determined.
出处
《特种橡胶制品》
北大核心
2000年第4期5-8,共4页
Special Purpose Rubber Products
