摘要
将高效薄层色谱 (TL C)分离技术和表面增强拉曼散射技术 (SERS)相结合 ,分析了中成药麻黄汤冲剂麻黄碱光谱 .研究表明 ,在 TL C原位约 8μg样品中可获得麻黄碱分子主要的振动特征谱带 ,并阐述了样品分子在表面增强基底吸附特征 ,从而阐朝了 TL C- SERS结合可对中成药主要化学成分进行高灵敏度的检测 .
A new method was developed to analyse the spectra of ephedrine in Chinese ephedra soup medicines,using surface\|enhanced technique to combine thin layer chromatographic (TLC) technique with surface\|enhanced Raman spectroscopy (SERS).The study indicates that the main vibrant characteristic spectral band of the ephedrine molecules can be obtained by TLC in the samples of about 8μg,and expounds characteristics of the sample molecules and the silica gel.Therefore,it's clarified that the main chemical composition of Chinese medicines can be carried as finger\|print type appraisal by combining TLC and SERS.\;
出处
《聊城师院学报(自然科学版)》
2000年第2期57-59,共3页
Journal of Liaocheng Teachers University(Natural Science Edition)
关键词
表面增强拉曼光谱
薄层色谱
麻黄碱
中草药
Surface\|enhanced Raman spectros,Thin\|layer chromatography,Fourier transform\|SERS,Ephedrine