摘要
以丁酮为起始原料,与盐酸羟胺反应生成丁酮肟,再与硫酸二乙酯反应得到丁酮肟乙基醚,在盐酸作用下水解得到乙氧胺,同时回收丁酮。收率为71.58%,纯度为99.33%。
Butanone oxime was synthesized by butanone and hydroxylamine hydro-chloride, and butanone oxiroe ethyl ether was prepared by butanone exime and diethyl sulfate. Ethoxyamine was gained by oxime ether.The butanone was recycled. The.yield was71.5% The purity was 99.33%.
出处
《浙江化工》
CAS
2012年第9期35-36,34,共3页
Zhejiang Chemical Industry
