摘要
对KY200型、LC—6型、RPA100型微库仑滴定仪测定石油产品硫含量的影响条件进行分析研究,测试不同品牌批号的碘化钾、冰乙酸所配电解液对试验的影响,确认碘化钾和冰乙酸的质量是造成仪器转化率低的主要因素,文中还讨论在测定不同浓度硫含量的油品时,电解液中有无叠氮化钠对测定的影响,并针对几起故障现象分析了原因。
This paper carried on the research analysis to the influence conditions on determi- nation of sulfur content in petroleum products by using different microcoulomb titrinuter. （KY2000, LC- 6, RPA100）. Having analysed the influence of different prepared electrolytes with different brands of potassium iodide , acetic acid indicated that the quality of potassium iodide, acetic acid was the primary factors leading to low conversion rate . This paper also discussed the effects of determination of different concentrations of sulfur content in petroleum products by electrolytes prepared without sodium azide ,and de reasons of several fault phenomena.
出处
《分析仪器》
CAS
2012年第4期75-78,共4页
Analytical Instrumentation
关键词
硫库仑法
电解液
叠氮化钠
石油
sulfur
coulometry
electrolytes
sodium azide
petroleum
