摘要
:将肌醇进行乙酰化衍生后得到肌醇六乙酯 ,然后用气相色谱法分析肌醇六乙酯 ,测得肌醇的含量。这种分析方法的变异系数为 0 .15% ,回收率为 98.2 %～ 10 4 .3%。方法简捷 。
Inositol was acetylated to inositol hexacetate and determined by GC. The content of inositol was got. The gas chromatographic conditions were as follows:2 m×3 mm i.d. column packed with 10%SE\|30/201 Diatoport PAW(60\|80 mesh) was kept at 240 ℃. The temperature of both injector and FID was 260 ℃. The flowrate of N\-2 carrier gas was 40 mL/min. The sample was analyzed by this method with a coefficient of variation of 0 15% and a recovery of 98 2%\|104 3%.
出处
《色谱》
CAS
CSCD
北大核心
2000年第3期265-266,共2页
Chinese Journal of Chromatography
基金
黑龙江省自然科学基金资助项目
