摘要
以液体喷射环流反应器为氧化反应装置,液相催化氧化芴制备芴酮。通过考察物料循环速度、反应温度、催化剂用量和溶剂的含水量等因素对芴酮收率的影响,得出最佳氧化反应条件。
The liquid-phase catalytic oxidation process for synthesizing fluorenone from fluorene is carried out in the liquid jet loop reactor （ LJLR ）. By investigating the influence of the rate of circulation of the material, the reaction temperature, the amount of catalyst and the water content in the solvent on the yield of fluorenone, the optimal reaction conditions are obtained.
出处
《现代化工》
CAS
CSCD
北大核心
2012年第6期77-79,共3页
Modern Chemical Industry
关键词
液体喷射环流反应器
芴
芴酮
氧化
liquid jet loop reactor
fluorene
fluorenone
oxidation
