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BDNPF/A增塑剂酸值的测定及评价 被引量:1

Determination and Evaluation on Acid Value of BDNPF/A Plasticizers
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摘要 采用电位滴定法和化学分析法测定BDNPF/A酸值,对这2种方法进行了精密度和准确度评价与比较。结果表明,这2种方法均可取得满意结果。对化学分析法的不确定度进行了评定和分析,经验证,滴定试样消耗的标准溶液体积对不确定度的贡献最大。 Acid value of BDNPF/A was determined by potentiometric titration method and chemical analysis method. The precision and accuracy of the two methods are evaluated and compared. The results show that the two methods can all obtain satisfied effects. The uncertainty of the chemical analysis method is evaluated and analyzed. It is verified that the contribution of the standard solution volume consumed for titrating sample on uncertainty is the largest.
机构地区 黎明化工研究院
出处 《化学推进剂与高分子材料》 CAS 2012年第3期92-97,共6页 Chemical Propellants & Polymeric Materials
关键词 BDNPF/A 酸值 测定 精密度 准确度 不确定度 BDNPF/A acid value determination precision accuracy uncertainty
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  • 1刘智敏,刘风.有关误差的基本概念与表示[J].宇航计测技术,1995,15(4):60-63. 被引量:6
  • 2姬月萍,李普瑞,汪伟,兰英,丁峰.含能增塑剂的研究现状及发展[J].火炸药学报,2005,28(4):47-51. 被引量:90
  • 3刘磊力,李凤生,杨毅,白桦萍.NiCu 复合金属粉的制备及其催化性能[J].过程工程学报,2007,7(1):155-159. 被引量:3
  • 4Kaplan R B, Shechter H. A new general reaction for preparing gem-dinitro compounds: Oxidative nitration [J]. JAm Chem Soc, 1961, 83(16): 3535-3536.
  • 5Eugene Guccione. Polaris gets improved fuel from new nitroplasticizers[J]. Chem Eng, 1963(7): 62-64.
  • 6Grakauskas Vytautas, Garver Lee C, Baum Kurt. Catalyzed oxidative nitration of nitronate salts[J]. J Org Chem, 1985, 50:1699-1 702.
  • 7Grakauskas Vytautas, Garver Lee C, Baum Kurt. Synthesis ofgeminal dinitro compounds: US, 4774336 [P]. 1988.
  • 8Grakauskas Vytautas, Garver Lee C, Baum Kurt. Synthesis ofgeminal dinitro compounds: US, 4910322 [P]. 1990.
  • 9Hamilton R Scott, Wardle Robert B. Synthesis ofbis (2,2-dinitropropyl) acetal(BDNPA): US, 5648556[P]. 1997.
  • 10Hamilton R Scott, Wardle Robert B. Synthesis ofbis (2,2-dinitropropyl) formal(BDNPF): US, 5449835[P]. 1995.

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