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微波和超声波提取脐橙皮渣总黄酮工艺条件优化 被引量:8

Process Optimization for Microwave-assisted and Ultrasonic-assisted Extraction of Total Flavonoids from Navel Orange Residue(Left over from Juicing)
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摘要 采用单因素试验及均匀设计法试验和SPSS 13.0统计软件回归分析,进行微波辅助和超声波辅助提取赣南脐橙皮渣中总黄酮的工艺研究。结果表明:微波辅助最佳提取条件为功率390W、辐射时间7min、乙醇体积分数50%、料液比1:45(g/mL),总黄酮提取可达19.3mg/g;超声波最佳提取条件为温度70℃、超声提取时间60min、乙醇体积分数50%、料液比1:45(g/mL),总黄酮提取可达16.6mg/g。 Based on one-factor-at-a-time experiments,uniform experimental design followed by regression analysis using the software SPSS 13.0 was carried out to optimize the microwave-assisted and ultrasonic-assisted extraction of total flavonoids from navel orange residue(left over from juicing).The optimal microwave-assisted extraction conditions were microwave power 390 W,irradiation time 7 min,ethanol concentration 50%,and material/liquid ratio of 1:45(g/mL) and the extraction rate of total flavonoids was 19.3 mg/g under these conditions.The optimal ultrasonic-assisted extraction conditions were temperature 70 ℃,ultrasonic treatment time 60 min,ethanol concentration 50%,and material/liquid ratio of 1:45(g/mL),and the resulting extraction rate of total flavonoids was 16.6 mg/g.
出处 《食品科学》 EI CAS CSCD 北大核心 2012年第6期19-23,共5页 Food Science
基金 江西省科技厅支撑计划项目(2010BNB1400) 江西省教育厅科学技术研究项目(GJJ10587) 江西省教育厅青年科学基金项目(GJJ11214) 赣州市果业基金项目(GZGY2008-1)
关键词 脐橙渣 微波辅助 超声波 总黄酮 navel orange residues microwave-assisted extraction ultrasonic-assisted extraction total flavonoids
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