摘要
萤石通过醋酸加热使ＣａＣＯ３ 溶解，再经过滤、沉淀、烘干，以碳酸钠、硼砂混合熔剂熔融，酸浸取后，采用 ＩＣＰ－ＡＥＳ法测定碳酸钙、氟化钙及二氧化硅、三氧化二铁。此方法精密度好，回收率在 ９６．０％ －１０１．４％ 之间。
The fluorite is heated in CH 3COOH to dissolve the CaCO 3 and then is filtered. The sediment is fused with Na 2CO 3 and Na 2B 4O 7, and then is converted into solution with HCl. Perfect analytic results about CaF 2,SiO 2,Fe 2O 3 can be obtained by ICP AES, the recovery is between 96.0% and 101.4%.
出处
《光谱实验室》
CAS
CSCD
2000年第1期115-117,共3页
Chinese Journal of Spectroscopy Laboratory
