摘要
用溶剂热法合成了两种金属卟啉,并探讨了目标化合物的合成条件。与常规加热的合成方法相比,溶剂热合成法具有操作简便、产物易分离提纯、产率高且能一步合成金属卟啉等优点。通过红外光谱、紫外可见光谱表征了目标化合物的结构,讨论了化合物的荧光性质。
The solvethermal synthesis of several metalloporphyrin was reported. The reaction condition was discussed Compared with conventional heating, solvethermal synthesis method has the advantages of simple operation,easy separa tion and purification,higher yield,and can synthesis metalloporphyrin in one step. The compound structures were charac tered by IR and UV-vis,its properties of FS were discussed.
出处
《武汉理工大学学报》
CAS
CSCD
北大核心
2011年第10期33-36,共4页
Journal of Wuhan University of Technology
基金
湖北省自然科学基金(2007ABA064)
湖北省教育厅重大科研项目基金(Z200727001)
关键词
卟啉
金属卟啉
溶剂热合成
光谱表征
porphyrins
metalloporphyrin
solvethermal synthesis
spectrum characterization
