摘要
The title compound exo-4-（3,4-dichlorophenyl）-8-ethyl-3,3a,4,5,8,12d-hexahydro-2H-furo[3,2-c]indolo[3,2-f]quinoline （C25H22Cl2N2O, Mr = 437.35） was synthesized and crystallized. The crystal belongs to tetragonal, space group I4（1）/a with a = 17.4903（3）, b = 17.4903（3）, c = 28.3403（5） , Z = 16, V = 8669.6（3） 3, Dc = 1.340 g·cm-3, μ（MoKɑ） = 0.319 mm-1, F（000） = 3648, R = 0.0429 and wR = 0.711 for 2714 observed reflections I 2σ（I）. X-ray analysis reveals that atoms C（1）, C（2）, C（3）, C（4）, C（5） and N（1） on the new pyridine ring are slightly distorted, forming a distorted boat conformation.
The title compound exo-4-（3,4-dichlorophenyl）-8-ethyl-3,3a,4,5,8,12d-hexahydro-2H-furo[3,2-c]indolo[3,2-f]quinoline （C25H22Cl2N2O, Mr = 437.35） was synthesized and crystallized. The crystal belongs to tetragonal, space group I4（1）/a with a = 17.4903（3）, b = 17.4903（3）, c = 28.3403（5） , Z = 16, V = 8669.6（3） 3, Dc = 1.340 g·cm-3, μ（MoKɑ） = 0.319 mm-1, F（000） = 3648, R = 0.0429 and wR = 0.711 for 2714 observed reflections I 2σ（I）. X-ray analysis reveals that atoms C（1）, C（2）, C（3）, C（4）, C（5） and N（1） on the new pyridine ring are slightly distorted, forming a distorted boat conformation.
基金
supported by the National Natural Science Foundation of China (20802061)
Natural Science Foundation of the Education Committee of Jiangsu Province (08KJD150019)
Qinglan Project (08QLT001) of the Education Committee of Jiangsu Province
