摘要
以丁基罗丹明Ｂ与锗钼杂多酸形成的三元配合物，测定了对冠心病有较好疗效的蒙药“心室Ⅱ”中锗的含量。提出了高灵敏度测定痕量锗的新方法，显色体系的表观摩尔吸光系数为５．６×１０＾５Ｌ／ｍｏｌ·ｃｍ，锗含量在０～７μｇ／２５ｍｌ范围内服从比尔定律，回收主继９６％～１０６％。
This paper describes the spectrophotometric determination of trace Ge in Mongolian drug' Ventricle Ⅱ' that has better curative possibilities for a coronary heart disease by the reducing of a ternary complex between butyl rhodamine B and Ge-Mo heteropoly acid.The molar absorptivity is 5.6×105 I/mol·cm.Beer Law is obeyed over the rang of 0 ~ 7 μg/25 mL for Ge.Owing to being added a suitable amount of alcohol,the sensitivity of the reaction is increased,and recovery is in the range of 96% ~ 106%.
出处
《化学分析计量》
CAS
1999年第1期23-24,共2页
Chemical Analysis And Meterage
基金
内蒙古高等学校科研基金
