摘要
通过系统研究,改进了四苯骈卟啉锌的纯化和脱锌的方法,发现用浓硫酸脱锌时绿色物质的生成与温度有关. 纯化方法经改进,产率和纯度均有所提高.
The synthesis of zinc(Ⅱ) tetrabenzporphyrin was reviewed and the purifying method of product was improved. Some questions about demetalization, including the cause that green substance present and factors that effect purifying, were explored. By improving, the green substance no longer yield.\;
出处
《武汉大学学报（自然科学版）》
CSCD
1999年第6期833-834,共2页
Journal of Wuhan University(Natural Science Edition)
基金
教育部博士点专项基金!(9448606)
国家自然科学基金!(29871024
29773033)
关键词
四苯骈卟啉锌
纯化
脱锌
合成
ZnTBP
H2TBP
tetrabenzporphyrin zinc(Ⅱ)
tetrabenzporphyrin
purify
demetalization of tetrabenzporphyrinate Zinc(Ⅱ)
