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高效液相色谱-蒸发光散射检测器测定芦荟西洋参软胶囊中的芦荟苷和人参皂苷Rb1、Rg1和Re含量

In highly effective liquid chromatography - evaporation light scattering detector determination aloe American ginseng soft capsule aloe glucoside and ginseng soap glucoside Rb1,Rg1 and Re content
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摘要 建立了高效液相色谱法-蒸发光散射检测器法(HPLC-ELSD)测定芦荟西洋参软胶囊中芦荟苷和人参皂苷Rb1、Rg1和Re含量测定方法.C18柱;流动相为乙腈-水(22∶78,甲酸调pH.至2.2);流速0.8mL/min;芦荟苷、人参皂苷Re、Rb1、Rg1在.2~1.2μg.ml-1的范围内呈良好的线性关系,回收率均在96.8~102.1%之间,RSD均低于3.6%;结果准确可靠,适用于该产品的质量控制. Has established in the highly effective liquid phase chromatography - evaporation light scattering detector law (HPLC- ELSD) determination aloe American ginseng soft capsule the aloe glucoside and ginseng soap glucoside Rhl, Rgl and the Re content determi- nation method. Cl8 column;The flowing for second grade nitrile - water (22.. 78, formic acid adjusts pH. to 2.2);Speed of flow 0. 8mL/ min;Aloe glucoside, ginseng soap glucoside Re, Rb1 , Rg1 in. 2- 1.2μg. rn1-1 scope assumes the good linear relations, the returns-ratio between 96.8-102. 1% ,RSD is lower than 3.6% ;Result accurate reliable,is suitable in this product quality control.
作者 宋明侠
机构地区 山东临沂大学
出处 《按摩与康复医学》 2011年第3期3-4,共2页 Chinese Manipulation and Rehabilitation Medicine
关键词 芦荟西洋参软胶囊 芦荟苷 人参皂苷RB1 人参皂苷RG1 人参皂苷RE Aloe American ginseng soft capsule Aloe glucoside Ginseng soap glucoside Rhl Ginseng soap glucoside Rgl Ginseng soap glucoside Re
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