摘要
目的:探讨吐根中醚溶性生物碱的提取方法。方法:采用正交实验法,以吐根中醚溶性生物碱的提取率为评价指标,考察提取工艺。结果:吐根中醚溶性生物碱的最佳提取条件为粉碎为10目,提取2次,每次12倍90%乙醇提取1小时。结论:该方法能充分有效的提取醚溶性生物碱,可作为吐根药材提取醚溶性生物碱的优选工艺。
Objective:To explore the technology in extraction of Ipecac. Methods:Experiment was designed by orthogonal design,taking the recovery rate of ether-soluble alkaloid as the observing indexes to investigate the extraction process. Resuh:The optimal decocting condition was as follow:Ipecac be crushed to 10 mesh, adding 12-fold 90% ethyl alcohol and hot reflux tow time per one hour. Conclusion:The optimal technique used in our investigation can thoroughly extract the ether-soluble alkaloid from Ipecac.
关键词
吐根
醚溶性生物碱
正交实验
Ipecac
ether-soluble alkaloid
Orthogonal Experiment