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石墨烯载钴材料的制备 被引量:4

Preparation of Graphene-supported Co Nanocomposite
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摘要 本实验以150μm鳞片状石墨为原料,采用Humm ers法制备氧化石墨,经超声波振荡得到氧化石墨烯,加入水合肼回流制得石墨烯材料。氧化石墨烯与CoSO4溶液混合,采用功能离子预吸附的方式,将金属离子有效地分散在氧化石墨烯载体上,原位还原金属颗粒和石墨烯,制备石墨烯载钴材料。 Graphite oxide is prepared by Hummers method using 150 μm flake graphite as raw materials,and further treated with super-sonic oscillation to get grapheme oxide.After hydrazine hydrate was added,grapheme oxide was reduced to graphene by reflux.Graphene oxide was mixed with CoSO4,and treated with hydrazine hydrate to obtain graphene supporting Co nanoparticles by reflux.
出处 《硅酸盐通报》 CAS CSCD 北大核心 2011年第1期98-100,共3页 Bulletin of the Chinese Ceramic Society
基金 高等学校博士点专项科研基金(20100143120012) 中央高校基本科研业务费专项资金资助(2010-Ⅳ-080) 国家"十一五"支撑计划项目(2008BAE60B08)
关键词 鳞片状石墨 氧化石墨 石墨烯 石墨烯载钴粒子 flake graphite graphite oxide graphene graphene-supported Co nanocomposite
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  • 1刘首鹏,周锋,金爱子,杨海方,马拥军,李辉,顾长志,吕力,姜博,郑泉水,王胜,彭练矛.人工裁剪制备石墨纳米结构[J].物理学报,2005,54(9):4251-4255. 被引量:11
  • 2张辉,张镇,姚运喜,谭大力,包信和.铂纳米团簇在修饰的HOPG表面的生长及性能表征[J].电子显微学报,2006,25(4):287-292. 被引量:4
  • 3GEIMA K, NOVOSELOOKS. The rise of graphene [ J ]. Nature Materials, 2007, (6) : 183 - 191.
  • 4KS NOVOSELOV, D JIANG, F SCHEDIN. Two-dimensional atomic crystals[J] . Proceedings of the National Academy of Sciences,2005,102(30): 10451 - 10453.
  • 5NOVOSELOOKS, GEIM A K, MOROZOVSV, et al. Electric field effect in atomically thin carbon films [J] . Science, 2004, (306) : 666 - 669.
  • 6NOVOSELOOKS, GEIM A K, MOROZOVSV, et al. Two- dimensional gas massless irac fermions in graphene [ J ]. Nature, 2005, (438) : 197 - 200.
  • 7ZHANGYB, TAN YW, STORMER HL, et al. Experimental observations of the quantum Hall effect and Berry's phase in graphene [J]. Nature,2005, (438): 201 - 204.
  • 8SIMONE PISANA, MICHELE LAZZERI, CINZIA CASIRAGHI. Born - Oppenheimer breakdown in graphene [J] . Nature Materials,2007 (6) : 198 - 201.
  • 9J GONZAILEZ, F GUINEA, MAH VOZMEDIANO. Electron - electron interactions in graphene sheets [J]. Physical Review B, 2001,63 (13) : 134421 - 1- 134421 - 8.
  • 10IGOR F HERBUT. Interactions and phase transitions on graphene's honeycomb lattice [J] . Physical Review Letters,2006,97 (14).

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  • 1傅玲,邹艳红,刘洪波,何月德.氧化石墨及其聚合物纳米复合材料的研究现状[J].炭素技术,2005,24(2):21-26. 被引量:13
  • 2Min S X,Wang F,Han Y Q.An investigation on synthesis and photocatalytic activity of polyaniline sensitized nanocrystalline TiO2 composites[J].J.Mater.Sci.,2007,42(24):9966-9972.
  • 3Pan X L,Fan Z L,Chen W,et al.Enhanced ethanol production inside carbon-nanotube reactors containing catalytic particles[J].Nat.Mater.,2007,6(7):507-511.
  • 4Zhang H,Fu Q,Yao Y X,et al.Size-dependent surface reactions of Ag nanoparticles supported on highly oriented pyrolytic graphite[J].Langmuir.,2008,24(19):10874-10878.
  • 5Zhang J,Liu X,Blume R,et al.Surface-modified carbon nanotubes catalyze oxidative dehydrogenation of n-butane[J].Science,2008,322(5898):73-77.
  • 6Geim A K,Novoselov K S.The rise of graphene[J].Nat.Mater.,2007,6:183-191.
  • 7Liu Z, Liu J Q, Cui L, et al. Preparation of graphene/polymer composites by direct exfoliation of graphite in functionalised block copolymer matrix[ J]. Carbon, 2013, 51 : 148 - 155.
  • 8Kakaei K. One-pot electrochemical synthesis of graphene by the exfoliation of graphite powder in sodium dodecyl sulfate and its decoration with platinum nanoparticles for methanol oxidation [ J ]. Carbon, 2013, 51 : 195 -201.
  • 9Ong B K, Poh H L, Chua C K, et al. Graphenes Prepared by Hummers, Staudenmaier and Hofmann Methods for Analysis of TNT- Based Nitroaromatic Explosives in Seawater [ J ]. Electroanalysis, 2012, 24(11) : 2085 -2093.
  • 10Min K, Han T H, Kim J, et al. A facile route to fabricate stable reduced graphene oxide dispersions in various media and their transparent conductive thin films [ J ]. Journal of Colloid and Interface Science, 2012, 383 : 36 - 42.

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