摘要
以甲基二氯硅烷、烯丙基氯和环己胺为原料、经过硅氢化反应、醇解反应和胺化反应合成了γ-环己胺丙基三乙氧基硅烷和甲基、γ-环已胺丙基二甲氧基硅烷.并用元素分析、IR和1H-NMR对它们作了表征.证实它们是新颖的有机硅偶联剂,可在纺织工业上制作柔软剂.
With methyldichlorosilane, allyl chloride and cyclohexamine used as rawmalerials, Methyl, γ -cyclohexaminopropyldimethoxysilane, Methyl γ -cyclohexaminopropyldiethoxysilanl, γ -cyclohexamino propyltriethoxysilane and γ -cyclohexaminopropyltrimethoxysilane were synthesized by silahydrogenization,esterification and amination. They were characterized by means of elemental analysis, IR and 1H-NMR.They are novel coupling agent of silane, In the weave industry they are used as softening agent.
出处
《南京师大学报(自然科学版)》
CAS
CSCD
1999年第1期64-67,72,共5页
Journal of Nanjing Normal University(Natural Science Edition)
基金
江苏省教委自然科学基金
关键词
偶联剂
柔软剂
织物
环己胺丙基硅烷
合成
Silahydrogenizatien Aminoalkylsilane Coupling agent, softening agent.