摘要
在对氯苯乙酮缩氨基硫脲(HL)为配体的非水溶剂中,以Cu,Fe,Zn金属做阳极,首次用电化学金属阳极氧化法合成了对氯苯乙酮缩氨基硫脲(HL)与Cu(Ⅰ),Fe(Ⅱ),Zn(Ⅱ)的金属配合物,通过元素分析、红外光谱、紫外光谱。
The metal complexes of Cu (Ⅰ), Fe(Ⅱ), Zn(Ⅱ) were synthesized by the electrochemical oxidation method of Cu,Fe, Zn anodic metal in non aqueoussolvent containing p chloroacetophenone thiosemicarbazone. The complexes were characterized by elemental analysis,IR,UV and molar conductivity.
出处
《宁夏大学学报(自然科学版)》
CAS
1999年第1期65-67,共3页
Journal of Ningxia University(Natural Science Edition)
基金
甘肃省自然科学基金
关键词
电化学合成
对氯苯乙酮
缩氨基硫脲
配合物
铜
electrochemical synthesis
p
chloroacetophenone thiosemicarbazone
organometallic complex