摘要
本文探索了以自蔓延高温(SHS)法合成并经抗水化处理的AlN粉为原料,添加YLiO_2-CaF_2/YLiO_2-CaCO_3的AlN陶瓷的低温烧结.研究表明,YLiO_2-CaF_2/YLiO_2-CaCO_3是有效的低温烧结助剂,添加5wt%YLiO_2和0.5wt%CaF_2。,在1675℃下保温6h可得到密度为3.29g/cm3、热导率为97w/m.K的中等性能的AlN陶瓷.同时对YLiO_2-CaF2、YLiO_2-CaCO3两种添加剂系统进行了对比研究.结果表明,在同样的烧结条件下,前者对AlN陶瓷的低温烧结更为有利.
The paper studied low-temperature sintering of Y-Li-Ca-Doped anti-hydrolysis AIN powderssynthesized by SHS method. It is found that Y-Li-Ca additive systems are beneficial for lowtemperature sintering of AIN ceramics. AlN samples with density of 3.29g/cm3 and thermalconductivity of 97 W/m.K were obtained after sintering at 1675℃ for 6 h with the additionsof 5wt% YLio2 and 0.5wt% CaF2. The work also indicates that YLiO2-CaF2 is better for lowtemperature signering of AIN than YLiO2-CaCO3 under the same sintering conditions.
出处
《无机材料学报》
SCIE
EI
CAS
CSCD
北大核心
1999年第1期175-179,共5页
Journal of Inorganic Materials