摘要
以4二甲基氨基吡啶(DMAP)为催化剂,使炔诺酮和醋酐反应,直接得到炔诺酮17醋酸酯.经熔点。
By the use of 4 dimethylaminopyridine as acylation catalyst,the norethisterone 17β acetate was synthesized by the direct reaction of norethisterone and acetic anhydride.It′s structure was confirmed by IR,UV, 1H NMR and mp.
出处
《中国药物化学杂志》
CAS
CSCD
1999年第1期59-60,共2页
Chinese Journal of Medicinal Chemistry