摘要
目的:建立鸡蛋花药材中反式苦橙油醇的含量测定方法。方法:采用气相色谱内标法,以十四醇为内标,测定鸡蛋花药材中反式苦橙油醇的含量。结果:反式苦橙油醇在0.0363~0.7250mg/ml范围呈良好的线性关系(r=0.9999),平均加样回收率为100.4%,RSD=0.63%。结论:气相色谱法测定反式苦橙油醇的含量,准确度高且重复性好,可作为鸡蛋花药材的质量控制方法之一。
Objective: To establish a method for the determination of d-nerolidol in Mexican Frangipani by GC. Methods: Tetradecyl alchohol served as the internal standard, GC method was used to determine the content of d-nerolidol in Mexican Frangipani. Results: The linear ranges of d-nerotidol was at 0.036 3-0.7250 mg/ml (r=0.999 9), the average recovery was 100.4% with a RSD of 0.63%. Conclusion: The method is accurate, reproducible, and can be used to control the quality of Mexican Frangipani.
出处
《中国医药导报》
CAS
2010年第13期57-58,共2页
China Medical Herald