摘要
在微波辐射下合成Ｎ芳基和Ｎ杂环取代氰乙酰胺，产率达８３％～９５％．反应是在经过改进的容器中进行的，容器置于频率为２４５０ＭＨｚ的微波炉中，常压下６～１０ｍｉｎ即可完成反应，反应速度快，后处理方便．
N substituted aryl and heterocycle cyanoamides are synthesized under microwave radiation, with the yields 83%～95%. The reaction is carried out in an improved container which is put into a microwave oven at 2 450 MHz. The reaction can be finished within 6￣10 min under normal pressure. The products can also be very conveniently treated.
出处
《扬州大学学报（自然科学版）》
CAS
CSCD
1998年第2期17-20,共4页
Journal of Yangzhou University：Natural Science Edition
基金
江苏省教委自然科学基金
关键词
微波辐射
氰乙酰胺
合成
芳基
杂环取代基
cyanoacetic acid(P)+acetamide(P)+aromatic amines(P)+primary amides
microwave radiation
amidation
