摘要
以乙醇胺为原料,经成盐、氯化、取代、加成和酯化等5步反应合成了二甲氨乙基二硫代氨基甲酸甲酯,总收率为50.6%。
S-Methyl-( N, N-dimethyl-amino )-ethyl-amino-dithiocarbamate was synthesizde from ethanolamine by hydrochlorination,hlorinatio, substitution addition and esterification. The overall yield of the 5 steps is 53 % .
出处
《广东化工》
CAS
1998年第4期22-23,共2页
Guangdong Chemical Industry
关键词
二甲氨乙基
二硫代氨基
甲酸甲酯
抗菌素
中间体
ethanolanline, 2 - chloro - ethylamine, N, N - dimethylethylenediamine S - methyl - (N, N-dimethyl - amino) - ethyl - amino - dithiocarbamate, synthesis