摘要
采用水热法成功合成了ZrSiO4/Cd(S1–xSex)包裹色料,通过X射线衍射、透射电子显微镜、红外光谱及色度测试研究了合成条件对色料性能的影响。结果表明:当水热反应温度为180℃,保温时间为10h,ZrSiO4/Cd(S1–xSex)=2时,色料具有较好的结晶度和色度,粒子细小且均匀,其尺寸分布为20～30nm。
An inclusion pigment of ZrSiO4/Cd（S1-xSex） was synthesized by a hydrothermal method. The effects of the synthesis pa- rameters （such as temperature, duration and molar ratio of ZrSiO4 to Cd（S1-xSex）） on the pigment properties were investigated by X-ray diffraction, transmission electron microscopy, infrared spectroscopy and chromaticity. The results show that the products in the particle size range of 20-30 nm with good crystallinity/intense hues and the narrow size distribution can be obtained in a molar ratio of ZrSiO4 to Cd（S1-xSex） of 2 and at a synthesis temperature of 180℃ for 10h.
出处
《硅酸盐学报》
EI
CAS
CSCD
北大核心
2009年第7期1264-1267,共4页
Journal of The Chinese Ceramic Society
基金
科技部国际科技合作计划(2005DFBA028)资助项目
教育部国家大学生创新实验计划(LA08025)资助项目
关键词
硅酸锆/硫硒化镉
包裹色料
水热合成
zircon cadmium sulfo-selenide
inclusion pigments
hydrothermal synthesis
