摘要
用反相高效液相色谱法在２０ｍｉｎ内同时测定化妆品中１１种防晒剂。色谱柱为ＹＷＧ－Ｃ１８柱，流动相为甲醇－四氢呋喃－水－高氯酸（２００２００１６００．１，Ｖ／Ｖ），检测波长为３１１ｎｍ。报告了对１０３种防晒化妆品测定的结果。
A method for quantitative determination of eleven sunscreen agents (benzophenone 4,p amino benzoic acid, salicylic acid, benzophenone 3,phenyl salicylate, 4 methylbenzylidene camphor, octyl dimethyl p amino benzoate, isopropyl dibenzoylmethane, butyl methoxydibenzoylmethane, octyl methoxycinnamate, octyl salicylate)in cosmetic products is described. It was based on a high performance liquid chromatographic separation under the condition of isocratic elution with a mixture solution of methanol THF water 70% perchloric acid (200∶200∶160∶01) by using a column packed with 10μm YWG C18 and UV detection. The recoveries (n=6) were 941% 101% and the relative standard deviations(n=6) for all eleven sunscreen agents were less than 5%. In addition, the results of analysis of 30 samples out of 103 samples of commercial suntan cosmetics performed are reported in this paper.
出处
《色谱》
CAS
CSCD
北大核心
1998年第3期223-225,共3页
Chinese Journal of Chromatography
基金
国家卫生部资助
关键词
高效液相色谱
防晒剂
化妆品
测定
分析
high performance liquid chromatography, sunscreen agents, cosmetics
