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Synthesis and Crystal Structure Analysis of 2-(3,5-Di-tert-butyl-2-hydroxyphenyl)-2-(3,4- dimethylphenyl) Acetic Acid Dimethylamine Salt

Synthesis and Crystal Structure Analysis of 2-(3,5-Di-tert-butyl-2-hydroxyphenyl)-2-(3,4- dimethylphenyl) Acetic Acid Dimethylamine Salt
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摘要 A new compound 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-2-(3,4-dimethylphenyl) acetic acid dimethylamine salt ([NH2(CH3)2][C24H31O3]) was synthesized and structurally determined. It is of monoclinic system, space group P21/c with a = 14.731(2), b = 10.1185(10), c = 17.065(2) A^°, β = 98.293(10)° ,Z = 4, V = 2517.0(6)A^°^3, Dc = 1.091 g/cm^3, F(000) = 904 and Mr= 413.58. The dihedral angle defined by two benzene rings is 98.23°. A new compound 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-2-(3,4-dimethylphenyl) acetic acid dimethylamine salt ([NH2(CH3)2][C24H31O3]) was synthesized and structurally determined. It is of monoclinic system, space group P21/c with a = 14.731(2), b = 10.1185(10), c = 17.065(2) A^°, β = 98.293(10)° ,Z = 4, V = 2517.0(6)A^°^3, Dc = 1.091 g/cm^3, F(000) = 904 and Mr= 413.58. The dihedral angle defined by two benzene rings is 98.23°.
出处 《Chinese Journal of Structural Chemistry》 SCIE CAS CSCD 2009年第4期414-418,共5页 结构化学(英文)
基金 supported by the Technology Risk Innovation Fund of PetroChina Company Ltd.
关键词 2-(3 5-di-tcrt-butyl-2-hydraxyphenyl)-2-(3 4-dimethylphenyl) acetic acid dimethylamine salt synthesis X-ray diffraction crystal structure 2-(3,5-di-tcrt-butyl-2-hydraxyphenyl)-2-(3,4-dimethylphenyl) acetic acid dimethylamine salt, synthesis, X-ray diffraction, crystal structure
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