摘要
以生产香兰素主要副产物──对二甲氨基苯胺为原料，通过缩合、环化等方法，以大于70％总收率合成标题化合物．并用元素分析、色谱-质谱联用、红外光谱及1HNMR谱等观测手段，对所合成的化合物进行表征．
The title compound was originally synthesized in an overall yield of more than 70% from p-dimethylamino-aniline the main by-product for producing vanillin by means of condensation and cyclization. The compound, being a white needle crystal with m. p. is 224~226℃, was characterized by means of elementary analysis, GC-Mass spectrum, IR spectrum and 1H NMR spectrum.
出处
《吉林大学自然科学学报》
CAS
CSCD
1998年第2期107-108,共2页
Acta Scientiarum Naturalium Universitatis Jilinensis
