摘要
本文合成了六个1-(N-芳基呋喃甲酰胺)亚甲基-2,8,9-三氧杂-5-氮杂-1-硅杂三环[3.3.3.O^(1.5)]十一烷的化合物。合成方法简便,反应时间短.易于后处理.经元素分析,IR,~1H NMR,MS确定了新化合物的结构.并经化合物3的X射线晶格衍射分析确定了该类化合物的空间排布情况。
Six 1-(N-arylfuroy, amidomethyl)-2,8, 9 -trioxa-5-aza-1-silatricyclo[3.3.3.O^(1'5)] undecanes 2—7 were synthesized. Their structures were established by elemental analysis, IR, ~1H NMR, MS. The crystal structure of 3 was studied by X-ray diffraction analysis.
出处
《化学学报》
SCIE
CAS
CSCD
北大核心
1990年第5期511-515,共5页
Acta Chimica Sinica
