摘要
采用两种方法合成了α-呋喃丙烯酸与有机钒配合物双(α-呋喃丙烯酸)氧钒,并对该配合物的合成方法进行了改进,对其结构进行了表征。方法一:由VOSO4和α-呋喃丙烯酸在水溶液中直接反应制得;方法二:由VOSO4和α-呋喃丙烯酸钡发生沉淀反应制得。结果表明,方法一的产率更高。
α-Furylacrylic acid and bis（α-furylacrylic alid） oxovanadium complex were designed and synthe-sized. The synthesis of bis（α-furylacrylic acid） oxovanadium complex was improved and explored with two methods. In aqueous solution, this compound was synthesized with VOSO4 and a-furylacrylic acid directly by the first method; this compound was synthesized with VOSO4 and α-furylacrylic acid barium by the second method. The yield of the first method was higher.
出处
《化学与生物工程》
CAS
2008年第8期10-11,共2页
Chemistry & Bioengineering
基金
河南工业大学引进人才资助项目(150207)
关键词
Α-呋喃丙烯酸
氧钒配合物
合成
α-furylacrylic acid
oxovanadium complex
synthesis
