摘要
利用一锅法合成标题化合物,并考察了溶剂浓度、物料配比、反应温度、反应时间及不同卤代烃对标题化合物产率的影响,将其产率由经典方法的30%～50%提高到90%以上。
S-Benzyldithiocarbazate has been synthesized by the one-pot batch process and the effect of ethanol concentration,proportion of raw materials,reaction temperature and reaction time on product yield was studied.The yield of S-benzyldithiocarbazate under the optimum condition was increased from 30%～50% to above 90%.
出处
《化学试剂》
CAS
CSCD
北大核心
2007年第11期684-686,共3页
Chemical Reagents
