摘要
以季戊四醇和三氯氧磷为原料,在微波条件下合成季戊四醇双磷酰氯,此方法与其他方法相比显著降低了反应温度,加快了反应速度,提高了反应收率。分析结果确证反应产物为目标产物。
Pentaerythritol phosphonyl dichloride was prepared from phosphoryl chloride and pentaerythritol by microwave irradiation.Result showed that reaction temperature and time were reduced and structure of the product was supported by analytical date.
出处
《云南化工》
CAS
2007年第4期17-20,共4页
Yunnan Chemical Technology
关键词
微波条件
季戊四醇双磷酰氯
合成
microwave irradiation
phosphonyl dichlororide
synthesis
