摘要
用凝胶法合成了［Ｎａ（１５Ｃ５）］２［Ｃｏ（ＮＣＳ）４（Ｈ２Ｏ）２］和［Ｎａ（１５Ｃ５）］２［Ｃｒ（ＮＣＳ）４（ＯＨ）（Ｈ２Ｏ）］两种配合物的单晶体，对它们进行了熔点测定、元素分析、红外光谱分析和热分析，对分析结果进行了讨论。
The single crystals of 2[Co(NCS) 4(H 2O) 2]and 2[Cr(NCS) 4(OH)(H 2O)] were obtained by gel method. Their composition and properties were determined by elemental analysis, melting point measurement, IR spectra and DTA methods. The testing results were discused.
出处
《山东科学》
CAS
1997年第1期40-43,共4页
Shandong Science
关键词
冠醚
配合物
合成
碱金属离子
物性
单晶
crown ether complex
sodium
cobalt
chromium
crystal grownth
