摘要
在超声波辐射条件下合成了N-苄基邻苯二甲酰亚胺,并且研究了影响反应产率的各种因素。实验得出最佳反应条件为:反应温度80℃,反应时间为30 min,反应产率达到95.3%。产物结构由元素分析、核磁共振氢谱确证。
N-phenmethyl phthalimide has been synthesized under ultrasound irradiation. Various factors affecting the yield have been studied. The optimum conditions have been obtained as follows:if reaction time is 30 min and reaction temperature 80℃, the yield of product will be 95.3 %. The structures are identified by elemental analysis and H NMR.
出处
《廊坊师范学院学报》
2007年第3期38-39,共2页
Journal of Langfang Teachers College