摘要
以异硫氰酸苯酯为原料,设计合成了6个新的α,ω-二(1-苯基-1,2,3,4-四氮唑-5-硫代)烷烃类化合物,其结构经元素分析、MS和1HNMR确认,并对其质谱裂解途径进行了探讨。
Six novelα,ω-bis （ 1-phenyl-1, 2, 3, 4-tetrazole-5- thio） alkane derivatives have been designed and synthesized based on the starting material isothiocyanatobenzene. All compounds synthesized were characterized by elementary analyses,^1HNMR, and MS, and the fragmentation mechanism of MS spectra was discussed as wall.
出处
《化学试剂》
CAS
CSCD
北大核心
2007年第2期91-93,共3页
Chemical Reagents
关键词
四氮唑
双硫醚
微波辐射
合成
表征
tetrazole
disulphide
microwave irradiation
synthe- sis
characterization
