摘要
本文研究了以环戊二烯和其它含有碳碳双键的化合物为原料,通过Diels-Alder反应,合成了降冰片烯类化合物:5-苯基-2-降冰片烯、5-腈基-2-降冰片烯、5-羧基-2-降冰片烯。实验应用了气相色谱仪(GC)、傅立叶变换红外光谱仪(FT-IR)、气相色谱-质谱联用仪(GC-MS)对产物进行了表征,取得了满意的结果。
By Using cyclopentadiene and carbon=carbon bond compounds as raw materials, based on Diels-Alder reaction, norbomene derivatives were prepared, such as 5-phenyl -2-nobomene, 5-cyano-2- nobomene, 5-carboxyl-2- nobomene and 5-nobomene-2- hydroxybutyrate. Gas Chromatography （GC）, Fuorier Transform Infrared Spectrometer （FT-LR）, Gas Chromatography- mass spectrometric （GC-MS） characterized all the compounds above, and the result is consonant with the target compounds.
出处
《邢台职业技术学院学报》
2007年第1期46-47,76,共3页
Journal of Xingtai Polytechnic College
基金
河南省杰出人才创新基金。编号:0421001300
