摘要
对α-紫罗兰酮合成的环化剂和溶剂进行了筛选.对合成的工艺条件(环化剂与溶剂的用量、反应时间、反应温度)进行了优化,在优化工艺条件下,紫罗兰酮的得率可达80%以上,α-紫罗兰酮的相对含量为80%左右.
Several solvents and catalysts ar compared and the technological conditions including the quantity of solvents and catalysts,the time and the temperature of the reaction are optimized.The yield of ionones is above 80% containing 80% α-isomer under the optimum conditions.
出处
《福州大学学报(自然科学版)》
CAS
CSCD
1996年第6期100-103,共4页
Journal of Fuzhou University(Natural Science Edition)