期刊文献+

偏钛酸常温水解沉淀法制备纳米TiO_2粉体的研究 被引量:1

PREPARATION OF NANO-TiO_2 POWDERS BY HYDROLYZATION-PRECIPITATION METHOD IN NORMAL TEMPERATURE BY THE USE OF THE MET TITANIC ACID AS THE MATERIALS
在线阅读 下载PDF
导出
摘要 以偏钛酸为原料通过常温水解-沉淀法制备了纳米TiO2粉体,用XRD和TEM等手段对粉体的晶型和形貌进行表征。用甲基橙为目标降解物,研究了其对甲基橙的降解性能,当分散剂加入量为13.5wt%,氨水溶液的pH值为4.0时得到的光催化剂粉体的晶粒尺寸均匀,粒径为10~20nm,其降解甲基橙的效率最高。 Nano-TiO2 powders were prepared with metatitanic acid as the initial materials by hydrolyzation-precipitation method in normal temperature and were characterized with XRD and TEM. The photocatalytic properties of nano-TiO2 were researched by degradating the methyl orange. The result shows that the degradation rate is the most obvious in degradating the methyl orange when using 13.5wt% of HPC as dispersant and adjusting the pH of the solution for 4.0.
作者 钟文建
出处 《中国陶瓷》 CAS CSCD 北大核心 2007年第1期27-29,共3页 China Ceramics
基金 长沙市科技局科技计划项目 编号:051036-12
关键词 光催化 纳米二氧化钛 水解沉淀法 Photocatalytic, nano-TiO2 powder, Hydrolyzation-Precipitation Method
  • 相关文献

参考文献8

  • 1张世英,周武艺,唐绍裘.液相法制备纳米二氧化钛陶瓷粉体的研究现状及其应用前景[J].陶瓷学报,2003,24(2):116-119. 被引量:27
  • 2LUSVARDI VS, BARREAU MA and FARNETH W E," The Effects of Bulk Titania Crystal structure on The Adsorption and Reaction of Aliphatic-Alcohols" [J].J.Catal. 1995, 153(1).41-53.
  • 3周武艺,唐绍裘,张世英,周锡荣,万隆.制备不同稀土掺杂的纳米氧化钛光催化剂及其光催化活性[J].硅酸盐学报,2004,32(10):1203-1208. 被引量:55
  • 4Yamashita. H, Harada. M, Misaka. J, et al. photocatalytic degradation of organic compounds diluted in water using visible light responsive metal ion-implanted TiO2 catalysts.Felon-implanted TiO2 [J] . catalysis Today. 2003,84(4): 191-196
  • 5ZELTNER WA,.HILL CG and ANDERSON MA,"Supported Titania for Photodegradation" [J].Chemtech,1993, 23(5): 21-28
  • 6HWANG SJ and RAFTERY D, "In Situ Solid state NMR Studies of Ethanol Photocatalysis. Characterization of Surface Sites and Their Reactivities" [J]. Catal,Today. 1999, 49(4):353-361
  • 7SZcZEPANKIEWICZ SH, COLUSSI AJ and HOFFMANN MR, "Infrared Spectra of Photoinduced Species on Hydroxylated Titania Surfaces" [J]. J. Phys,Chem B. 2000, 104(42):9842-9850
  • 8JEAN JH and RING TA, "Processing Monosized TiO2 Powders Generated with HPC Dispersant" [J]..Am,Ceram. Soc. Bull.1986,65(12).1574-1577

二级参考文献24

  • 1沈兴海,高宏成.纳米微粒的微乳液制备法[J].化学通报,1995(11):6-9. 被引量:102
  • 2高濂,陈锦元,黄军华,严东生.醇盐水解法制备二氧化钛纳米粉体[J].无机材料学报,1995,10(4):423-427. 被引量:82
  • 3顾达,何碧,胡黎明.相转移法制备高纯超细TiO_2技术研究[J].压电与声光,1995,17(5):45-48. 被引量:11
  • 4陈代荣,孟祥建,李博,孙思修.偏钛酸作前驱体水热合成TiO_2微粉[J].无机材料学报,1997,12(1):110-114. 被引量:58
  • 5[1]LINSEBIGLER A L,LU G ,YATES J R,et al.Photocatalyst on TiO2 surfaces: principles,mechanisms and selected results .Chem Rev,1995,95:735-758.
  • 6[2]WANG R,HASHIMOTO K,FUJISHIMA A,et al.Light-induced amphiphilic surface .Nature,1997,388:431-432.
  • 7[3]HADJIIVANOV K I,KLISSURSKI D K.Surface chemistry of titania and titaniua-supported catalysts .Chem Rev,1996,25:61-69.
  • 8[4]FUJISHIMA A,RAO T,TRYK D.Titanium dioxide photo catalysis .J Photochem Photobio C: Photochem Rev,2000,1:1-21.
  • 9[5]HOFFMANN M R,MARTIN S T,CHOI W,et al.Environmental applications of semiconductor photo catalysis .Chem Rev,1995,95(1): 69-96.
  • 10[6]ASAHI R,MORIKAWA T,OHWAKI T,et al.Visible-light photo catalysis in nitrogen-doped titanium oxides .Science,2001,293(13): 269-271.

共引文献80

同被引文献40

引证文献1

二级引证文献4

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部