摘要
本文报道利用简单的溶剂热方法,以相应的金属盐作为唯一的反应物来制备Ag,Cu,Cd,Ni等纳米结构金属。采用XRD,SEM,TEM等测试手段对产物进行了表征。实验结果表明,反应条件特别是反应时间对产物最后的化学组成起重要作用。该制备方法具有一定的普适性,而且简单实用;涉及的反应条件相对温和,获得的产物具有双亲性质,能均匀分散于大部分极性和非极性溶剂中。
Nanostructured Ag, Cu, Cd, Ni were synthesized using the corresponding metal salts as mono-precursors via a facile solvothermal method, and the products were characterized by XRD ,SEM and TEM. It is proved that the reaction time plays a key role in determining the composition of the products. This simple and general process is environment-friendly, and the products obtained are amphiphilic and dispersible well in most of the polar and nonpolar solvents.
出处
《无机化学学报》
SCIE
CAS
CSCD
北大核心
2006年第8期1401-1405,共5页
Chinese Journal of Inorganic Chemistry
基金
国家自然科学基金资助项目(No.20331010)
关键词
溶剂热法
过渡金属
纳米结构
双亲
solvothermal
transition metal
nano-structure
amphiphilic
