摘要
建立了氟菌唑的高效液相色谱分析方法。采用250mm×4.0mmLichrosobRP-185μmMERCK色谱住,238nm紫外检测器。以乙腈-缓冲溶液(60+40V/V)为流动相,流速为1.5ml/min,该方法处理简单、快速、准确、适用,方法线性范围为1.6￣2.4mg/ml,回收率为99.4%￣100.5%,变异系数为0.25%。
A method was developed for analyzing triflumizole by HPLC using a 250 × 4.0 mm, 5pro Merck Lichrosob RP-18 chromatographic column with 238 nm UV detection. The mobile phase was acetonitrile-buffer solution （60：40 by vol） and flow rate was 1.5 ml/min. The method was simple, rapid, accurate, and practical. Range of linearity was 1.6～2.4 mg/ml, recovery was 99.4～100.5%, and the coefficient of variation was 0.25%.
出处
《农药》
CAS
北大核心
2006年第4期259-260,共2页
Agrochemicals
关键词
氟菌唑
乙腈
磷酸二氢钾
磷酸
triflumizole
acetonitrile
potassium dihydrogen phosphate
phosphoric acid
