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甲苯氯化合成氯化苄的毛细管色谱分析 被引量:2

Capillary chromatography analysis on benzyl chloride chlorinated synthesis by methylbenzene
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摘要 采用自制的0.25mm×30m×0.5μmPEG-20M(聚乙二醇-20000)高效石英毛细管色谱柱建立了甲苯的色谱分析方法。用自制的0.25mm×30m×0.5μmOV-1701毛细管色谱柱建立了氯化苄的色谱分析方法。所建方法明显优于标准GB/T3144-82(甲苯)和HG/2027-91(氯化苄)内的方法,具有分离效果好,分析速度快,重复性好的优点。 Chromatography analysis method of methylbenzene were established by 0.25 mm×30 m× 0.5 μmPEG-20M high efficiency self-made quartz capillary chromatographic column. Chromatography analysis method of benzyl chloride were established by 0.25 mm×30 m×0.5μmOV-1701 self-made capillary chromatographic column. This above methods are better than the methods mentioned in the standard of GB/T3144-82 and HG/2027-91. The method has some advantages, including the efficiency of segregation and repeatability is good, and analytical velocity is quickly.
出处 《中国氯碱》 CAS 2006年第2期27-29,共3页 China Chlor-Alkali
关键词 甲苯 氯化苄 毛细管气相色谱 PEG-20M OV-1701 methylbenzene benzyl chloride capillary gas chromatography PEG-20 OV-1701
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参考文献6

  • 1HG/2027-91.工业氯化苄.[S].,..
  • 2张莘民,徐朝,李爱强.气相色谱法测定废水中的氯化苄[J].环境科学与技术,1999(4):48-49. 被引量:8
  • 3Sun T H,Cao L K,Jia J P. Novel activated carbon fiber solid-phase microextraction for determination of benzyl chloride and related compounds in water by gas chromatography-mass spectrometry.Chromatographia, 2005, (61): 173-179
  • 4张莘民,徐朝,李爱强,程滢.气相色谱法测定环境空气中氯化苄和甲苯[J].环境监测管理与技术,2000,12(3):33-34. 被引量:5
  • 5Frost R P,Hussain M S,Raghani A R. Determination of pharmaceutical process impurities by solid phase microextraction gas chromatography.Journal of Separation Science, 2003, (26): 1097-1103
  • 6GB/T3144—82.甲苯中烃类杂质的气相色谱法.[S].,..

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