摘要
用反相高效液相色谱法测定了吴茱萸及制剂中吴茱萸碱和吴茱萸次碱，建立了中药及制剂中吴茱萸碱、吴茱萸次碱分离、测定的色谱方法。色谱条件：ＯＤＳ柱，乙腈＋水＋四氢呋喃＋乙酸（５２＋４８＋１＋０．１）为流动相，紫外检测波长２８０ｎｍ。方法简便、灵敏、准确、快速。
A RP-HPLC method for determination of evodiamine and rutaecarpine in fructus evodae, a Chinese herbal medicine, and its preparation was established. The chromatographic conditions are listed below: ODS column, UV detector at wavelenth 225nm, and a mobile phase composed of acetonitrile+water+THF+acetic acid(52+48+1+0. 1).
出处
《分析测试学报》
CAS
CSCD
1996年第3期60-62,共3页
Journal of Instrumental Analysis
关键词
吴茱萸
吴茱萸碱
吴茱萸次碱
高效液相色谱
Evodia rutaecarpa(Juss.) Benth., Evodiamina, Rutaecarpine, HPLC.
