摘要
用溶剂汽油、萘烷、石油醚按一定比例复配成混合型溶剂,以对茴香胺为原料,用该溶剂合成了3磺酸基对茴香胺,产品中不含致癌物.产品收率在82%以上,溶剂回收率在95%以上.
The mixed solvent consists of solvent naphtha,decalin,and petroleum ether in a certain proportion,which was used to synthesize 3-sulfo p-anisidine by using p-anisidine as raw material. The yield of prouduct was over 82 % ,and there was no carcinogenic compound in the product,and the recovery of solvent was over 95 %.
出处
《河北师范大学学报(自然科学版)》
CAS
北大核心
2006年第1期73-74,82,共3页
Journal of Hebei Normal University:Natural Science
基金
河北省科学技术厅星火计划项目(04123023)