摘要
以[N(Bu)4]Br为相转移催化剂,用于α-氯代正了基异了基醚与无水乙酸钠之间的亲核取代反应,首次合成了1-异丁氧基-1-正丁酸乙酸酯,产率达60.2%。该化合物具有清新愉快的甜香气,富有浓郁自然特色。
In this paper, [N(Bu)4]Br was applied to the nucleophilic substitution reaction of α-chlorobutyl isobutyl ether with anhydrous sodium acetate,a new perfume compound 1-isobutoxybutyl acetate was synthesized, the yields reached up to 60. 2%. The product is with navour sweet aroma and numerous natural features.
出处
《化学试剂》
CAS
CSCD
北大核心
1996年第1期41-42,共2页
Chemical Reagents
基金
河南省教委资助课题